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The first announcement of the discovery of element was announced by physicists at the Nobel Institute in Sweden in The team reported that they had bombarded a curium target with carbon ions for twenty-five hours in half-hour intervals.

Between bombardments, ion-exchange chemistry was performed on the target. Twelve out of the fifty bombardments contained samples emitting 8. In , the Swedish team attempted to explain the Berkeley team's inability to detect element in , maintaining that they did discover it.

This hypothesis is lent weight by the fact that thorium can easily be produced in the reaction used and would not be separated out by the chemical methods used.

Later work on nobelium also showed that the divalent state is more stable than the trivalent one and hence that the samples emitting the alpha particles could not have contained nobelium, as the divalent nobelium would not have eluted with the other trivalent actinides.

The Berkeley team, consisting of Albert Ghiorso , Glenn T. Seaborg , John R. They were unable to confirm the 8. In , the Berkeley team attempted to defend their work, stating that the isotope found was indeed Fm but the isotope that the half-life measurements actually related to was californium, granddaughter of , produced from the more abundant curium Energy differences were then attributed to "resolution and drift problems", although these had not been previously reported and should also have influenced other results.

However, work also showed that the Fm recoil could have also easily been produced from the isomeric transition of m Fm half-life 1. In , the team continued their studies and claimed that they were able to produce an isotope that decayed predominantly by emission of an 8.

The activity was initially assigned to but later changed to However, they also noted that it was not certain that nobelium had been produced due to difficult conditions.

Meanwhile, in Dubna, experiments were carried out in and aiming to synthesize element as well. The first experiment bombarded plutonium and with oxygen ions.

Some alpha decays with energies just over 8. Later experiments proved that these were background effects.

In , Berkeley scientists claimed the discovery of element in the reaction of californium with boron and carbon ions. They assigned this to without giving a reason for the assignment.

The values do not agree with those now known for No, although they do agree with those now known for No, and while this isotope probably played a part in this experiment, its discovery was inconclusive.

Work on element also continued in Dubna, and in , experiments were carried out there to detect alpha-decay daughters of element isotopes by synthesizing element from the reaction of a uranium target with neon ions.

The products were carried along a silver catcher foil and purified chemically, and the isotopes Fm and Fm were detected. The yield of Fm was interpreted as evidence that its parent was also synthesized: as it was noted that Fm could also be produced directly in this reaction by the simultaneous emission of an alpha particle with the excess neutrons, steps were taken to ensure that Fm could not go directly to the catcher foil.

In hindsight, the Dubna results on were probably correct and can be now considered a conclusive detection of element In , the Dubna team carried out chemical experiments on element and concluded that it behaved as the heavier homologue of ytterbium.

In , the IUPAC - IUPAP Transfermium Working Group TWG reassessed the claims of discovery and concluded that only the Dubna work from correctly detected and assigned decays to nuclei with atomic number at the time.

The Dubna team are therefore officially recognised as the discoverers of nobelium although it is possible that it was detected at Berkeley in In , as part of an attempted resolution to the element naming controversy, IUPAC ratified names for elements — For element , it ratified the name nobelium No on the basis that it had become entrenched in the literature over the course of 30 years and that Alfred Nobel should be commemorated in this fashion.

In the periodic table , nobelium is located to the right of the actinide mendelevium , to the left of the actinide lawrencium , and below the lanthanide ytterbium.

Nobelium metal has not yet been prepared in bulk quantities, and bulk preparation is currently impossible. The lanthanides and actinides, in the metallic state, can exist as either divalent such as europium and ytterbium or trivalent most other lanthanides metals.

In , Johansson and Rosengren examined the measured and predicted values for the cohesive energies enthalpies of crystallization of the metallic lanthanides and actinides , both as divalent and trivalent metals.

It took nineteen years before this prediction was confirmed. In , experiments were conducted to compare nobelium's chemical behavior to that of terbium , californium , and fermium.

All four elements were reacted with chlorine and the resulting chlorides were deposited along a tube, along which they were carried by a gas.

It was found that the nobelium chloride produced was strongly adsorbed on solid surfaces, proving that it was not very volatile , like the chlorides of the other three investigated elements.

However, both NoCl 2 and NoCl 3 were expected to exhibit nonvolatile behavior and hence this experiment was inconclusive as to what the preferred oxidation state of nobelium was.

This proved that in aqueous solution, nobelium is most stable in the divalent state when strong oxidizers are absent.

This occurs because of the large energy gap between the 5f and 6d orbitals at the end of the actinide series. The long No—H distances in the NoH 2 molecule and the significant charge transfer lead to extreme ionicity with a dipole moment of 5.

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2 Kommentare

  1. Gukora

    Bemerkenswert, diese sehr wertvolle Mitteilung

  2. Monos

    Talentvoll...

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